FLUORAT®-02-series Analyzers |
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Appearance
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FLUORAT®-02, which was a pioneering instrument developed by LUMEX
and have gained a wide use in many analytical laboratories, makes
a baseline for a number of analytical fluorometric, photometric, and
chemoluminometric techniques. This versatility allows an analyst to
choose the optimal method for assaying each component being determined.
The Fluorat analyzers embody the modular principle. The base unit,
FLUORAT®-02, is a filter fluorometer, chemiluminometer and photometer
implemented together in the same optoelectronic scheme, whereas the
FLUORAT®-02-2M version is, in addition, a time-resolving fluorometer
and can also be used as a fluorometric detector in any HPLC system,
relevant measuring cells being interchangeable.
FLUORAT-02 is an automated analyzer furnished with a package of certified
methods for monitoring the quality of drinking and waste water in
compliance with sanitary Regulations, as well as for assaying a number
of air, soil, and food product constituents. The analytical methods
implemented using this instrument are chosen so that to reliably detect
half of the prescribed UTC and to provide the simplest sample preparation.
For example, it takes 2 to 3, 5 to 7, and 2 to 3 minutes, respectively,
to prepare a sample of petroleum hydrocarbons, phenols, and surfactants
for analysis.
Wide spectral range
FLUORAT®-02 analyzer is equipped with a high-pressure xenon arc lamp,
which emits high-intensity light in a spectral range from 200 to 950
nm.
Versatility
The instrument is basically a fluorometer, however, it can be also
operated as a photometer, chemiluminometer, or phosphorimeter. The
cell compartment accommodates 10x10 mm cells for fluorometry, or 10x20
and 10x40 mm cells for photometry (the latter two in the FLUORAT®-02-2M
model).
Use in the field
The analyzer is energized from AC mains or from a 12-V accumulator
battery, which allows its use in mobile laboratories.
Automated operation procedures
The names of the methods, result processing technique, and calibration
coefficients are displayed in the user's menu. The menu content and
the loaded calibrations are stored in a nonvolatile memory. The self-diagnostics
procedure is automatically performed when the instrument is switched
on and during measurement. When carrying out an analysis, an operator
merely chooses the necessary method from the menu and, having installed
a cell, starts measuring. The concentration of a component being measured
is indicated on a built-in LC display or is transmitted via a serial
port to a standalone computer for further processing.
The table above lists the detection limits for some substances in
analysis of water using FLUORAT®-02 analyzers in compliance with the
certified methods. It should be noted that these methods are optimized
for reliable identification of UTCs, the actual detection limits being
lower than those given in the table.
Water. Detection limits (DL)
| PERFORMANCE CHARACTERISTICS
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| Fluorescent
methods |
DL (mg/l) |
sample volume,
ml |
| petroleum hydrocarbons |
0.005 |
100 |
| phenols |
0.0005 |
250 |
| anionic surfactants |
0.025 |
5 |
| cationic surfactants |
0.01 |
5 |
| formaldehyde |
0.002 |
25 |
| nitrites |
0.005 |
5 |
| nitrates |
0.1 |
5 |
| sulfides |
0.005 |
10 |
| fluorodes |
0.01 |
10 |
| copper |
0.005 |
2 |
| zinc |
0.005 |
50 |
| arsenic |
0.001 |
100 |
| cadmium |
0.0005 |
200 |
| selenium |
0.0001 |
100 |
| beryllium |
0.0005 |
1000 |
| stannum |
0.01 |
10 |
| boron |
0.05 |
5 |
| aluminum |
0.01 |
10 |
| cobalt |
0.0001 |
25 |
| iron |
0.05 |
10 |
| nickel |
0.01 |
100 |
| Chemiluminescent
methods |
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| chromium (total) |
0.002 |
2 |
| Phosphorescent
methods |
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| uranium* |
0.0002 |
5 |
| Cryoluminescent
methods |
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| benzo[a]pyrene*
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0.000001 |
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| lead* |
0.001 |
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Notes: *) only for FLUORAT®-02-2M model
FLUORAT®-02-3M and FLUORAT®-02-2M analyzer versions
FLUORAT®-02-2M enables measuring the phosphorescence intensity,
operating in the time-resolving fluorometer mode. This mode is used
for the detection of uranium, featuring very high sensitivity and
selectivity. The analyzer can also operate with a fiber optic bundle,
which allows measuring luminescence or reflected light from the surface
of an outside sample, such as paper, cathodoliminophors, etc. FLUORAT®-02-2M
can be combined with CRYO-1/2 attachment and can also be used as a
fluorometric detector for HPLC systems.
FLUORAT®-02-02/3M features:
- operation in custom menu mode to analyze standard list contaminants
- saving calibration tables and background value for 16 different
components in the built-in memory
- printout of analysis results
- storing results in the built-in memory
- energized from AC mains or from a 12-V accumulator battery
- self-diagnostics: the device
automatically identifies failures in all units
| SPECIFICATIONS |
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02-3M |
02-2M |
| Spectral range |
200 - 1000 nm
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200-650 nm |
| Cell types |
Q10, Q20, Q40
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Q10, Q20, Q40 |
| Power requirements |
220
Vac, 50 Hz; 12 Vdc, 36 W |
| Size |
300x300x90 mm |
330x300x120 mm |
| Weight |
8 kg |
10 kg |
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